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Abstract

The development of competent green chemistry methods for synthesis of metal nanoparticles have become a main limelight of researchers in the field of nanotechnology.Nanoparticles are advanced matarials have recently gained high attention due to their scientific and technological important. They find awide variety of applications such as catalysts with huge activity and specificity,metal semiconductor In this thesis, preparation compound ( CuFe2O4@SiO2-PA-TFA MNPs ) synthesized CuFe2O4@SiO2 functionalized with propylamine and trifluoroacetic acid. Heterocycle compounds are an important compound of organic chemistry that exist in the structure of natural products and are responsible for the biological and pharmacological properties of most medicinal compounds. Characterization of CuFe2O4@SiO2-PA-TFA MNPs was performed by SEM, EDX, XRD, TGA and VSM analysis. Application of these nanoparticles in the synthesis of tetrahydropyrazolopyridines, shown high activity of the catalyst.

Keywords

Trifluoroacetic CuFe2O4@SiO2 TFA propylamine

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This work is licensed under a Creative Commons Attribution-NonCommercial 4.0 International License.

How to Cite
Bushra Farhood Zwaid, Dr. Lotfi Shiri, & Ahmed abdul wahhab abdul sattar. (2022). Synthesis and Characterization of New nanoparticles compound. Texas Journal of Multidisciplinary Studies, 12, 7–13. Retrieved from https://zienjournals.com/index.php/tjm/article/view/2323

References

  1. A. Al-Mulla, Der Pharma Chemica, 9(13),141-147, (2017).
  2. A. Weissberger ,(Ed.),“The Chemistry of Heterocyclic Compounds”, Vols. 1 to 29, Wiley, New York (1950 to 1975).
  3. R. C. Elderfield ,(Ed.),“Heterocyclic Chemistry”, Vols. 1 to 9, Wiley, New York (1950 to 1967) .
  4. J. A. Joule and G. F. Smith, “Heterocyclic Chemistry”, 2 nd Eddition,Van Nostrand Reinhold Co., London (1978)
  5. O. Buchardt ,(Ed.), “Photochemistry of Heterocyclic Compounds”, Wiley, New York (1976) .
  6. S. Mora, S.Nagoriaa , S. Sindhua and V. Singhb, Chemistry and Biology Interface, 7(1) 1-18, (2017).
  7. Maleki, A.; Chalavand, R.; Firouzi Haji, R.; (2017) Applied Organometallic Chemistry, 31. DOI: 10.1002/aoc.3916.
  8. Armstrong, R. W.; Combs, A. P.; Tempest, P. A.; Brown, S. D.; Keating, T. A.; (1996) Accounts of Chemical Research, 29, 123.
  9. Mukhopadhyay, C.; Tapaswi, P. K.; Drew, M. G.; (2010) Tetrahedron Letters, 51, 3944.
  10. Yavari, I.; Moradi, L.; (2006) Tetrahedron letters, 47, 1627.
  11. Yavari, I.; Hossaini, Z.; Sabbaghan, M.; (2006) Tetrahedron letters, 47, 6037.
  12. Salehi, N.; Mirjalili, B. B. F.; (2018) Research on Chemical Intermediate, 44, 7065.
  13. Warshakoon, N. C.; Wu, S.; Boyer, A.; Kawamoto, R.; Renock, S.; Xu, K.; Pokross, M.; Evdokimov, A. G.; Zhou, S.; Winter, C.; Walter, R.; Mekel, M.; (2006) Bioorganic and Medicinal Chemistry Letters, 16, 5687.
  14. Tschammer, N.; Elsner, J.; Goetz, A.; Ehrlich, K.; Schuster, S.; Ruberg, M.; Kuhhorn, J.; Thompson, D.; Whistler, J.; Hubner, H.; Gmeiner, P.; (2011) Journal of Medicinal Chemistry, 54, 2477.
  15. Bare, T. M.; McLaren, C. D.; Campbell, J. B.; Firor, J. W.; Resch, J. F.; Walters, C. P.; Salama, A. I.; Meiners, B. A.; Patel, J. B.; (1989) Journal of Medicinal Chemistry, 32, 2561.
  16. Bettinetti, L.; Schlotter, K.; Hu¨bner, H.; Gmeiner, P.; (2002) Journal of Medicinal Chemistry, 45, 4594.
  17. De Mello, H.; Echevarria, A.; Bernardino, A. M.; Canto-Cavalheiro, M.; Leon, L. L.; (2004) Journal of Medicinal Chemistry, 47, 5427.
  18. Chioua, M.; Samadi, A.; Soriano, E.; Lozach, O.; Meijer, L.; Marco-Contelles, J.; (2009) Bioorganic and Medicinal Chemistry Letters, 19, 4566.
  19. Rostami, H.; Shiri, L.; (2021) Materials Today Chemistry, 20, 100400.
  20. Maleki, A.; Nooraie Yeganeh, N.; (2017) Applied Organometallic Chemistry, 31. https://doi.org/10.1002/aoc.3814.
  21. Maleki, A.; Chalavand, R.; Firouzi Haji, R.; (2017) Applied Organometallic Chemistry, 31. DOI: 10.1002/aoc.3916.
  22. Rostami, H.; Shiri, L.; (2020) Applied Organometallic Chemistry, 34, p.e5599.